Only if you directly connect to them, if you send a file or receive a file from the other person, you can use "netstat -a" on the command line and look for the port and ip that you are connected to. MSN only uses a certain port range for file transfers. This should make it easy to pick out the right IP.
Go to start, run, then type cmd for windows 2000 or xp or command for win98 or millenium, then hit ok. Now in the dos prompt type netstat -a and it will remain.
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